REGULATIONS (26:9 VA.R. January 4, 2010)

TABLE OF CONTENTS

Register Information Page

Publication Schedule and Deadlines

Petitions for Rulemaking

Notices of Intended Regulatory Action

Regulations

1VAC30-40. Regulations for the Certification of Laboratories Analyzing Drinking Water (Final)

2VAC5-70. Health Requirements Governing the Control of Equine Infectious Anemia in Virginia (Proposed)

2VAC5-316. Rules and Regulations for Enforcement of the Virginia Pest Law - Beach Vitex Quarantine (Final)

4VAC20-20. Pertaining to the Licensing of Fixed Fishing Devices (Final)

4VAC20-490. Pertaining to Sharks (Final)

4VAC20-610. Pertaining to Commercial Fishing and Mandatory Harvest Reporting (Final)

4VAC20-900. Pertaining to Horseshoe Crab (Final)

4VAC50-60. Virginia Stormwater Management Program (VSMP) Permit Regulations (Final)

4VAC50-60. Virginia Stormwater Management Program (VSMP) Permit Regulations (Final)

9VAC5-10. General Definitions (Fast-Track)

10VAC5-110. Credit Counseling (Final)

13VAC10-180. Rules and Regulations for Allocation of Low-Income Housing Tax Credits (Final)

14VAC5-310. Rules Governing Actuarial Opinions and Memoranda (Final)

14VAC5-321. Use of the 2001 CSO Mortality Table in Determining Reserve Liabilities and Nonforfeiture Benefits (Final)

20VAC5-317. Rates for Standby Service Furnished to Certain Renewable Cogeneration Facilities Pursuant to § 56-235.1:1 of the Code of Virginia (Final)

22VAC40-601. Food Stamp Program (Proposed)

23VAC10-210. Retail Sales and Use Tax (Final)

24VAC30-510. Frontage Roads (Final)

Governor

General Notices/Errata

 


REGISTER INFORMATION PAGE

The Virginia Register OF REGULATIONS is an official state publication issued every other week throughout the year. Indexes are published quarterly, and are cumulative for the year. The Virginia Register has several functions. The new and amended sections of regulations, both as proposed and as finally adopted, are required by law to be published in the Virginia Register. In addition, the Virginia Register is a source of other information about state government, including petitions for rulemaking, emergency regulations, executive orders issued by the Governor, the Virginia Tax Bulletin issued periodically by the Department of Taxation, and notices of public hearings and open meetings of state agencies.

ADOPTION, AMENDMENT, AND REPEAL OF REGULATIONS

An agency wishing to adopt, amend, or repeal regulations must first publish in the Virginia Register a notice of intended regulatory action; a basis, purpose, substance and issues statement; an economic impact analysis prepared by the Department of Planning and Budget; the agency’s response to the economic impact analysis; a summary; a notice giving the public an opportunity to comment on the proposal; and the text of the proposed regulation.

Following publication of the proposal in the Virginia Register, the promulgating agency receives public comments for a minimum of 60 days. The Governor reviews the proposed regulation to determine if it is necessary to protect the public health, safety and welfare, and if it is clearly written and easily understandable. If the Governor chooses to comment on the proposed regulation, his comments must be transmitted to the agency and the Registrar no later than 15 days following the completion of the 60-day public comment period. The Governor’s comments, if any, will be published in the Virginia Register. Not less than 15 days following the completion of the 60-day public comment period, the agency may adopt the proposed regulation.

The Joint Commission on Administrative Rules (JCAR) or the appropriate standing committee of each house of the General Assembly may meet during the promulgation or final adoption process and file an objection with the Registrar and the promulgating agency. The objection will be published in the Virginia Register. Within 21 days after receipt by the agency of a legislative objection, the agency shall file a response with the Registrar, the objecting legislative body, and the Governor.

When final action is taken, the agency again publishes the text of the regulation as adopted, highlighting all changes made to the proposed regulation and explaining any substantial changes made since publication of the proposal. A 30-day final adoption period begins upon final publication in the Virginia Register.

The Governor may review the final regulation during this time and, if he objects, forward his objection to the Registrar and the agency. In addition to or in lieu of filing a formal objection, the Governor may suspend the effective date of a portion or all of a regulation until the end of the next regular General Assembly session by issuing a directive signed by a majority of the members of the appropriate legislative body and the Governor. The Governor’s objection or suspension of the regulation, or both, will be published in the Virginia Register. If the Governor finds that changes made to the proposed regulation have substantial impact, he may require the agency to provide an additional 30-day public comment period on the changes. Notice of the additional public comment period required by the Governor will be published in the Virginia Register.

The agency shall suspend the regulatory process for 30 days when it receives requests from 25 or more individuals to solicit additional public comment, unless the agency determines that the changes have minor or inconsequential impact.

A regulation becomes effective at the conclusion of the 30-day final adoption period, or at any other later date specified by the promulgating agency, unless (i) a legislative objection has been filed, in which event the regulation, unless withdrawn, becomes effective on the date specified, which shall be after the expiration of the 21-day objection period; (ii) the Governor exercises his authority to require the agency to provide for additional public comment, in which event the regulation, unless withdrawn, becomes effective on the date specified, which shall be after the expiration of the period for which the Governor has provided for additional public comment; (iii) the Governor and the General Assembly exercise their authority to suspend the effective date of a regulation until the end of the next regular legislative session; or (iv) the agency suspends the regulatory process, in which event the regulation, unless withdrawn, becomes effective on the date specified, which shall be after the expiration of the 30-day public comment period and no earlier than 15 days from publication of the readopted action.

Proposed regulatory action may be withdrawn by the promulgating agency at any time before the regulation becomes final.

FAST-TRACK RULEMAKING PROCESS

Section 2.2-4012.1 of the Code of Virginia provides an exemption from certain provisions of the Administrative Process Act for agency regulations deemed by the Governor to be noncontroversial.  To use this process, Governor's concurrence is required and advance notice must be provided to certain legislative committees.  Fast-track regulations will become effective on the date noted in the regulatory action if no objections to using the process are filed in accordance with § 2.2-4012.1.

EMERGENCY REGULATIONS

Pursuant to § 2.2-4011 of the Code of Virginia, an agency, upon consultation with the Attorney General, and at the discretion of the Governor, may adopt emergency regulations that are necessitated by an emergency situation. An agency may also adopt an emergency regulation when Virginia statutory law or the appropriation act or federal law or federal regulation requires that a regulation be effective in 280 days or less from its enactment. The emergency regulation becomes operative upon its adoption and filing with the Registrar of Regulations, unless a later date is specified. Emergency regulations are limited to no more than 12 months in duration; however, may be extended for six months under certain circumstances as provided for in § 2.2-4011 D. Emergency regulations are published as soon as possible in the Register.

During the time the emergency status is in effect, the agency may proceed with the adoption of permanent regulations through the usual procedures. To begin promulgating the replacement regulation, the agency must (i) file the Notice of Intended Regulatory Action with the Registrar within 60 days of the effective date of the emergency regulation and (ii) file the proposed regulation with the Registrar within 180 days of the effective date of the emergency regulation. If the agency chooses not to adopt the regulations, the emergency status ends when the prescribed time limit expires.

STATEMENT

The foregoing constitutes a generalized statement of the procedures to be followed. For specific statutory language, it is suggested that Article 2 (§ 2.2-4006 et seq.) of Chapter 40 of Title 2.2 of the Code of Virginia be examined carefully.

CITATION TO THE VIRGINIA REGISTER

The Virginia Register is cited by volume, issue, page number, and date. 23:7 VA.R. 1023-1140 December 11, 2006, refers to Volume 23, Issue 7, pages 1023 through 1140 of the Virginia Register issued on December 11, 2006.

The Virginia Register of Regulations is published pursuant to Article 6 (§ 2.2-4031 et seq.) of Chapter 40 of Title 2.2 of the Code of Virginia.

Members of the Virginia Code Commission: R. Steven Landes, Chairman; John S. Edwards, Vice Chairman; Ryan T. McDougle; Robert Hurt; Robert L. Calhoun; Frank S. Ferguson; E.M. Miller, Jr.; Thomas M. Moncure, Jr.; James F. Almand; Jane M. Roush.

Staff of the Virginia Register: Jane D. Chaffin, Registrar of Regulations; June T. Chandler, Assistant Registrar.


PUBLICATION SCHEDULE AND DEADLINES

January 2010 through October 2010

Volume: Issue

Material Submitted By Noon*

Will Be Published On

INDEX 1 Volume 26

 

January 2010

26:9

December 15, 2009 (Tuesday)

January 4, 2010

26:10

December 29, 2009 (Tuesday)

January 18, 2010

26:11

January 13, 2010

February 1, 2010

26:12

January 27, 2010

February 15, 2010

26:13

February 10, 2010

March 1, 2010

26:14

February 24, 2010

March 15, 2010

INDEX 2 Volume 26

 

April 2010

26:15

March 10, 2010

March 29, 2010

26:16

March 24, 2010

April 12, 2010

26:17

April 7, 2010

April 26, 2010

26:18

April 21, 2010

May 10, 2010

26:19

May 5, 2010

May 24, 2010

26:20

May 19, 2010

June 7, 2010

INDEX 3 Volume 26

 

July 2010

26:21

June 2, 2010

June 21, 2010

26:22

June 16, 2010

July 5, 2010

26:23

June 30, 2010

July 19, 2010

26:24

July 14, 2010

August 2, 2010

26:25

July 28, 2010

August 16, 2010

26:26

August 11, 2010

August 30, 2010

FINAL INDEX Volume 26

 

October 2010

27:1

August 25, 2010

September 13, 2010

27:2

September 8, 2010

September 27, 2010

27:3

September 22, 2010

October 11, 2010

27:4

October 6, 2010

October 25, 2010

*Filing deadlines are Wednesdays unless otherwise specified.


PETITIONS FOR RULEMAKING

TITLE 12. HEALTH

STATE BOARD OF BEHAVIORAL HEALTH AND DEVELOPMENTAL SERVICES

Agency Decision

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Amend the regulations to require the reason documented for denying patient access to service records and criteria for removal to be consistent with the statement the physician is required to put into the service record in order to deny patient access to the same.

Agency Decision: Request denied.

Statement of Reason for Decision: The board determined that 12VAC35-115 provides adequate protections with respect to restrictions being placed on an individual access to his or her services record.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-04; Filed December 9, 2009, 3:55 p.m.

Agency Decision

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: The reinstatement of the requirement on limiting the timeframe of how long the provider can impose a restriction on the patient's access to their service records.

Agency Decision: Request denied.

Statement of Reasons for Decision: The board determined that 12VAC35-115 has never included a requirement limiting the length of time that a restriction could be placed on a patient's access to his or her service record. The board determined that to do so would be to regulate a clinical practice issue.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-05; Filed December 9, 2009, 3:55 p.m.

Agency Decision

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Regulation governing amendment of the service records should be amended to require the reviewer of patient requests to amend/correct their services records to be neither the patient's treating clinician nor a person who wrote the particular note in the service record that the patient is requesting to be amended/corrected.

Agency Decision: Request denied.

Statement of Reasons for Decision: The board determined that the existing provisions of 12VAC35-115 provide individuals receiving services with a clearly delineated right to have a statement of disagreement included in the record.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-06; Filed December 9, 2009, 3:55 p.m.

Agency Decision

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Regulation governing access to or amendment/correction of patients' service records should be amended to limit to 10 days from the date of the submission's request, (i) the physician's response to a patient's request for accessing his service record and (ii) the reviewer's response to a patient's request for amending/correcting his service record.

Agency Decision: Request denied.

Statement of Reasons for Decision: The board determined that 12VAC35-115 should not be changed to establish a specific timeframe within which a provider must respond to record access requests. Requirements regarding response timeframes are already established by state and federal laws and differ based on the type of provider.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-07; Filed December 9, 2009, 3:55 p.m.

Agency Decision

Title of Regulation: None specified.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Regulation governing different legal statuses of inpatient hospitalization and their discharge criteria should repeal the provision requiring or allowing a "provider" to wait until after 30 days from admission to inform the involuntarily, civilly committed patients' of their right to seek discharge from the facility director and their right to seek legal appeal of their civil commitment order to the Circuit Court pursuant to § 37.2-830 of the Code of Virginia.

Agency Decision: Request denied.

Statement of Reasons for Decision: The board determined that 12VAC35-115-70 B 8 b neither requires nor allows a provider to wait for 30 days after admission to notify the individual receiving services of his right to appeal an order of involuntary commitment.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-08; Filed December 9, 2009, 3:55 p.m.

Agency Decision

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Regulations allowing the commissioner to suspend the applicability of the human rights regulation, through a written exemption, to people on forensic status or civilly committed as sexually violent predators should be repealed.

Agency Decision: Request denied.

Statement of Reasons for Decision: The board determined that the authority granted under 12VAC35-115 to the commissioner to balance individual rights with the need for public safety is consistent with the provisions of § 37.2-400 of the Code of Virginia.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-09; Filed December 9, 2009, 3:55 p.m.

Agency Decision

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Regulation should be amended to prohibit the commissioner from suspending the applicability of provisions in the human rights regulations that apply to people on forensic status or civilly committed as sexually violent predators through a written exemption where there are duplicate provisions of the same rights in the statutes (§ 37.2-400 of the Code of Virginia).

Agency Decision: Request denied.

Statement of Reasons for Decision: The board determined that § 37.2-400 of the Code of Virginia does allow qualifications to the statutorily defined rights when such qualifications are consistent with reasonable limitations and sound therapeutic treatment.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-10; Filed December 9, 2009, 3:55 p.m.

 

Agency Decision

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Regulation should be amended to require the commissioner to specify the section codes and provisions as apart of the written exemptions for suspending the applicability of the human rights regulation to people on forensic status and civilly committed as sexually violent predators.

Agency Decision: Request denied.

Statement of Reasons for Decision: The board determined that the subject of this petition is adequately addressed in departmental policy guidance and does not require regulatory action.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-11; Filed December 9, 2009, 3:55 p.m.

Initial Agency Notice

Title of Regulation: 12VAC35-115. Rules and Regulations to Assure the Rights of Individuals Receiving Services from Providers Licensed, Funded, or Operated by the Department of Mental Health, Mental Retardation and Substance Abuse Services.

Statutory Authority: §§ 37.2-202 and 37.2-400 of the Code of Virginia.

Name of Petitioner: Steven Shoon.

Nature of Petitioner's Request: Adjust the complaint resolution process to remove the director or director's designee from handling the Human Rights Complaint when the director or director's designee's conduct, position, or circumstances renders them unable to perform an impartial review of the Human Rights Complaint. This includes prohibiting the director of appointing a designee for handling the Human Rights Complaint.

Agency's Plan for Disposition of the Request: The board will consider the petition and any comments received at its first meeting after the conclusion of the public comment period.

Comments may be submitted until January 25, 2010.

Agency Contact: Linda B. Grasewicz, Senior Planner, Department of Behavioral Health and Developmental Services, P.O. Box 1797, Richmond, VA 23218-1797, telephone (804) 786-0040, FAX (804) 371-0092, or email linda.grasewicz@dbhds.virginia.gov.

VA.R. Doc. No. R10-30; Filed December 10, 2009, 4:38 p.m.


NOTICES OF INTENDED REGULATORY ACTION

TITLE 4. CONSERVATION AND NATURAL RESOURCES

VIRGINIA SOIL AND WATER CONSERVATION BOARD

Notice of Intended Regulatory Action

Notice is hereby given in accordance with § 2.2-4007.01 of the Code of Virginia that the Virginia Soil and Water Conservation Board intends to consider amending the following regulations: 4VAC50-60, Virginia Stormwater Management Regulations. The purpose of the proposed action is to establish water quality design criteria for new development activities within the Chesapeake Bay Watershed that are consistent with the pollutant loadings called for in the Environmental Protection Agency-approved Virginia Total Maximum Daily Load (TMDL) Implementation Plan for the Chesapeake Bay Nutrient and Sediment TMDL, and consider compliance methodologies and mechanisms associated with any new design criteria.

The agency intends to hold a public hearing on the proposed action after publication in the Virginia Register.

Statutory Authority: §§ 10.1-107 and 10.1-603.4 of the Code of Virginia.

Public Comment Deadline: February 3, 2010.

Agency Contact: David C. Dowling, Policy, Planning, and Budget Director, Department of Conservation and Recreation, 203 Governor Street, Suite 302, Richmond, VA 23219, telephone (804) 786-2291, FAX (804) 786-6141, or email david.dowling@dcr.virginia.gov.

VA.R. Doc. No. R10-2265; Filed December 14, 2009, 3:23 p.m.

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TITLE 8. EDUCATION

STATE BOARD OF EDUCATION

Notice of Intended Regulatory Action

Notice is hereby given in accordance with § 2.2-4007.01 of the Code of Virginia that the State Board of Education intends to consider amending the following regulations: 8VAC20-120, Career and Technical Education Regulations. Changes in both federal and state laws pertaining to career and technical education have made it necessary to revise the Career and Technical Education Regulations. The regulations will be examined in their entirety, including the requirements for general provisions, administration of career and technical education programs, and operation of career and technical education programs. The goals of this review are to (i) update the regulations to comply with new state and federal laws, such as an identification and clarification of the U.S. Department of Education's approved Virginia requirements for meeting the performance standards of the Perkins Act of 2006; (ii) update definitions for consistency with state and federal regulations dealing with similar issues such as a clarification of "career clusters," "career pathways," "sustained professional development," and other terms impacted by the Perkins Act of 2006; and (iii) eliminate any duplication of regulations.

The agency intends to hold a public hearing on the proposed action after publication in the Virginia Register.

Statutory Authority: §§ 22.1-16 and 22.1-227 of the Code of Virginia.

Public Comment Deadline: February 8, 2010.

Agency Contact: Anne Rowe, Career and Technical Education Coordinator, Department of Education, P.O. Box 2120, Richmond, VA 23218, telephone (804) 225-2838, FAX (804) 371-2456, or email anne.rowe@doe.virginia.gov.

VA.R. Doc. No. R10-2244; Filed December 14, 2009, 2:01 p.m.

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TITLE 13. HOUSING

BOARD OF HOUSING AND COMMUNITY DEVELOPMENT

Notice of Intended Regulatory Action

Notice is hereby given in accordance with § 2.2-4007.01 of the Code of Virginia that the Board of Housing and Community Development intends to consider amending the following regulations: 13VAC5-112, Enterprise Zone Grant Program Regulation. The purpose of the proposed action is to enable the enterprise zone program to be administered in a more efficient and economical manner and to ensure that the regulations provide clear and understandable guidelines by addressing all issues concerning the performance of the program by (i) further clarifying the intent of the program and insuring that it is being met, (ii) providing additional guidance to program constituents, (iii) formalizing what has been common practice, and (iv) updating references to specific statutes and dates.

The agency intends to hold a public hearing on the proposed action after publication in the Virginia Register.

Statutory Authority: § 59.1-533 of the Code of Virginia.

Public Comment Deadline: February 3, 2010.

Agency Contact: Stephen W. Calhoun, Regulatory Coordinator, Department of Housing and Community Development, Main Street Centre, 600 E. Main Street, Suite 300, Richmond, VA 23219, telephone (804) 371-7000, FAX (804) 371-7090, TTY (804) 371-7089, or email steve.calhoun@dhcd.virginia.gov.

VA.R. Doc. No. R10-2174; Filed December 14, 2009, 2:02 p.m.


REGULATIONS

TITLE 1. ADMINISTRATION

DEPARTMENT OF GENERAL SERVICES

Final Regulation

REGISTRAR'S NOTICE: The following regulatory action is exempt from the Administrative Process Act in accordance with § 2.2-4006 A 4 c of the Code of Virginia, which excludes regulations that are necessary to meet the requirements of federal law or regulations, provided such regulations do not differ materially from those required by federal law or regulation. The Department of General Services will receive, consider, and respond to petitions by any interested person at any time with respect to reconsideration or revision.

Title of Regulation: 1VAC30-40. Regulations for the Certification of Laboratories Analyzing Drinking Water (amending 1VAC30-40-10, 1VAC30-40-20, 1VAC30-40-30, 1VAC30-40-40, 1VAC30-40-100, 1VAC30-40-110, 1VAC30-40-130, 1VAC30-40-150, 1VAC30-40-240, 1VAC30-40-250, 1VAC30-40-280, 1VAC30-40-320, 1VAC30-40-330, 1VAC30-40-340, 1VAC30-40-360, 1VAC30-40-370; adding 1VAC30-40-85).

Statutory Authority: §§ 2.2-1102 and 2.2-1105 of the Code of Virginia.

Effective Date: February 3, 2010.

Agency Contact: Rhonda Bishton, Regulatory Coordinator, Department of General Services, 1100 Bank Street, Suite 420, Richmond, VA 23219, telephone (804) 786-3311, FAX (804) 371-8305, or email rhonda.bishton@dgs.virginia.gov.

Summary:

Laboratories analyzing drinking water samples under the federal Safe Drinking Water Act (SDWA) must use current federal Environmental Protection Agency (EPA) approved test methods and adhere to other laboratory-specific requirements, as set out in 40 CFR Parts 141 and 143. The lists of test methods are revised regularly to include newly approved methods and delete out-of-date methods. These lists are also revised when new SDWA program requirements are promulgated in the Federal Register.

The changes to the Certification of Laboratories Analyzing Drinking Water Regulations conform them to current federal requirements for test methods, sampling, and laboratory certification.  1VAC30-40-85 is added to incorporate by reference the most current federal requirements. Out-of-date citations and out-of-date tables listing test methods and sample container, preservation, and holding time requirements are deleted. Provisions in the regulations that were taken verbatim from now out-of-date test methods and federal requirements are deleted and replaced by incorporating by reference current requirements. Finally, technical changes are made to replace the Division of Water Supply Engineering with the Office of Drinking Water to reflect the correct name of the Virginia Department of Health division responsible for these regulations.

Part I
General Provisions

1VAC30-40-10. Introduction.

The Safe Drinking Water Act (SDWA) of December 16, 1974, mandated the establishment of drinking water regulations. The United States Environmental Protection Agency (USEPA) was authorized to set the national drinking water regulations and oversee the implementation of the SDWA. State governments through their health departments or environmental agencies were to accept the responsibility for the implementation and enforcement of the SDWA'S provisions.

The Virginia Department of Health, Division of Water Supply Engineering (VDH-DWSE) Office of Drinking Water (VDH-ODW) has accepted and maintains the primary enforcement responsibility (primacy) under the SDWA and the requirements of the National Primary Drinking Water Regulations (NPDWR) 40 CFR 141, 142 and 143 (2009). The regulation at 40 CFR 141.28 requires that all testing for compliance purposes except turbidity, free chlorine residual, temperature and pH be performed by laboratories certified by the state.

The Department of General Services, Division of Consolidated Laboratory Services (DGS-DCLS) has been designated by VDH- DWSE VDH-ODW as the principal state laboratory. Pursuant to regulation 40 CFR 142.10(b)(3)(i) (2009), DGS-DCLS has established and maintains the state program for the certification of laboratories conducting analytical measurements of drinking water contaminants.

This chapter provides the mechanism to assure that laboratories are capable of providing valid data for compliance under the SDWA.

1VAC30-40-20. Definitions.

The following words and terms, when used in this chapter, shall have the following meanings, unless the context already indicates otherwise:

"Analyst" means a chemist, microbiologist, physicist, or technician who actually performs a test. The analyst may carry out the complete test or participate jointly with other analysts. The qualifications an analyst needs depend greatly on functions being performed.

"Certifying team" means experienced DGS-DCLS professionals to perform laboratory on-site evaluations under the SDWA.

"CFR" means Code of Federal Regulations.

"Compliance sample" means any sample required by the Virginia Department of Health to determine that the water quality does not exceed the maximum contaminant level (MCL) for each specified parameter.

"DGS-DCLS" means the Department of General Services-Division of Consolidated Laboratory Services.

"EMSL-LV" means the Environmental Monitoring Systems Laboratory in Las Vegas, Nevada.

"Maximum contaminant level (MCL)" means the maximum permissible level of a contaminant in water which is delivered to the free flowing outlet of the ultimate user of a waterworks.

"Minimum requirements" means criteria which are critical to the generation of valid data. These criteria describe the lowest level of capability at which the analyses can be successfully performed.

"NPDWR" means the National Primary Drinking Water Regulations (40 CFR 141 et seq.) (2009).

"Performance evaluation sample" means annual sample to be analyzed by a laboratory on certain parameters for which certification has been requested or granted. This annual sample is a form of documentation of a laboratory's capabilities in conjunction with on-site inspection evaluations of the laboratory by the certifying team.

"Primary enforcement responsibility (Primacy)" means the primary responsibility for administration and enforcement of primary drinking water regulations and related requirements applicable to public water systems within a state.

"Quality Assurance (QA) Plan" means a written description of a laboratory's quality assurance activities.

"SDWA" means the Safe Drinking Water Act (21 USCS § 349; 42 USCS §§ 201, 300f to 300j-9) (42 USC § 300 f et seq.).

"TTHM" means Total Trihalomethanes.

"USEPA" means the United States Environmental Protection Agency.

"VDH-DWSE" "VDH-ODW" means the Virginia Department of Health-Division of Water Supply Engineering Virginia Department of Health - Office of Drinking Water.

"Virginia laboratory officer" means the DGS-DCLS coordinator of drinking water laboratory certification activities.

1VAC30-40-30. Public notification for exceeded MCL.

The public notification regulations require that a laboratory analyzing compliance samples immediately notify the VDH-DWSE VDH-ODW of all results which exceed an MCL in accordance with Virginia Waterworks Regulations, 12VAC5-590-530 and 12VAC5-590-540, June 23, 1993; the Public Notification Final Rule, Federal Register Vol. 52, No. 208, October 28, 1987; and the Public Notification Technical Amendment, Federal Register Vol. 54, No. 72, April 17, 1989.

1VAC30-40-40. Compliance data report.

A. A waterworks with an on-site certified laboratory shall follow the reporting requirements outlined in Virginia Waterworks Regulations, VR 355-18-005.09, 2.20 Reporting, June 23, 1993 12VAC5-590-530.

B. A contract laboratory analyzing compliance samples shall complete the appropriate VDH-DWSE VDH-ODW Sample Input Form in accordance with the instructions for compliance under the SDWA. The contract laboratory shall report the analysis result to the VDH-DWSE VDH-ODW within three days of completion date of sample analysis.

1VAC30-40-85. Incorporation by reference.

A. The sampling, analytical methodology, and laboratory certification requirements of 40 CFR 141 and 143 (2009) are incorporated by reference into this chapter.

B. The specific sampling, analytical methodology, and laboratory certification requirements incorporated by reference are listed below by category:

1. Inorganic chemistry: 40 CFR 141.23, 40 CFR 141.89, and 40 CFR 141.131.

2. Organic chemistry: 40 CFR 141.24 and 40 CFR 141.131.

3. Microbiology: 40 CFR 141.21, 40 CFR 141.74, 40 CFR 141.174, 40 CFR 141.704, and 40 CFR 141.705. 40 CFR 136.3 (a) for e. coli requirements under 40 CFR 141.704.

4. Radiochemistry: 40 CFR 141.25.

5. Alternative testing methods: 40 CFR Part 141, Subpart C, Appendix A.

6. Test methods specified for secondary maximum contaminant levels: 40 CFR 143.4.

C. The exceptions to the requirements for laboratory certification in 40 CFR 141.28, 40 CFR 141.74(a), 40 CFR 141.89(a)(1), 40 CFR 141.131(b)(3), and 40 CFR 141.131(c)(3) are incorporated by reference into this chapter. Laboratory testing for alkalinity, calcium, conductivity, disinfectant residual, orthophosphate, pH, silica, temperature, and turbidity for compliance purposes may be performed by laboratories or persons not certified under this chapter but acceptable to VDH-ODW.

1VAC30-40-100. Evaluation procedure.

A. DGS-DCLS shall notify a laboratory three weeks before the on-site evaluation.

B. During the on-site evaluation, the certifying team shall evaluate the laboratory on its equipment and supplies, general laboratory practices, sample collection, handling and preservation, methodology and quality assurance. A laboratory may be required to analyze an unknown sample or perform analysis on a parameter during the evaluation.

Survey forms may be used as guidelines for complete coverage of the laboratory's activities. Each deviation observed during the laboratory evaluation shall be discussed at the time it is observed. The certifying team shall make an oral report to the laboratory staff at the end of the evaluation.

C. The certifying team shall prepare a narrative and action report for the Virginia laboratory officer. This report shall contain information pertinent to the evaluation. The report shall recommend the parameters in a category for which certification can be granted.

D. DGS-DCLS shall obtain from VDH-DWSE VDH-ODW an identification number for a newly certified laboratory. DGS-DCLS shall inform VDH- DSWE VDH-ODW of the certification status of a laboratory.

E. The Virginia laboratory officer shall advise the laboratory within 30 days after the on-site evaluation of its certification status and forward the certifying team's complete report.

F. Each laboratory found to be in noncompliance with this chapter, as indicated in the certifying team report, shall submit documentation of the corrective actions at the time specified by DGS-DCLS.

G. Additional actions toward certification shall be determined based on the specific circumstances.

1VAC30-40-110. Levels of certification.

Certification is granted for individual parameters in a category except for the volatile organic chemicals (VOC's). The VOC's are certified as a group based on the method employed and successful completion of the performance evaluation study.

1. "Certified" means a laboratory that meets the minimum requirements as determined by the certifying team using this chapter. The certification shall be valid for up to three years.

2. "Provisionally certified" means a laboratory which has deficiencies but can still produce valid data. The laboratory can continue to report compliance data to VDH-DWSE VDH-ODW. A laboratory shall be permitted up to six months for correction of deficiencies. The certifying team may perform an announced or unannounced on-site evaluation to determine the adequacy of documented corrective actions. The certifying team shall recommend to the Virginia laboratory officer to upgrade the laboratory's certification status.

3. "Not certified" means a laboratory that does not meet the minimum requirements as determined by the certifying team using this chapter.

1VAC30-40-130. Maintenance of certified status.

To maintain its certified status, a laboratory shall:

1. Continue to meet the requirements listed in this chapter based on the on-site evaluation.

2. Pass performance evaluation samples on an annual basis (for radiochemistry pass additional two cross-check samples).

3. Perform a minimum of five water analyses for each chemical parameter per month. Refer to 1VAC30-40-330 for the minimum number of microbiology analyses. This shall ensure that the laboratory maintains expertise in the certified categories.

4. Notify DGS-DCLS within 30 days of changes in personnel, equipment or laboratory location which may change the laboratory's analytical capability.

5. Use approved methodology listed in this chapter incorporated by reference at 1VAC30-40-85.

6. Notify VDH-DWSE VDH-ODW in accordance with 1VAC30-40-30.

1VAC30-40-150. Revocation of certified status.

A laboratory shall be downgraded from certified or provisionally certified to not certified status for:

1. Failure to employ USEPA approved methods incorporated by reference at 1VAC30-40-85.

2. Failure to submit report for the performance evaluation study at the specified time limit unless a waiver is approved by DGS-DCLS.

3. Failure to successfully analyze a parameter that is provisionally certified.

4. Submission of a performance evaluation sample to another laboratory for analysis and reporting the data as its own.

5. Failure to correct identified deficiencies based on an on-site visit.

6. Permitting persons other than qualified personnel to perform and report results for drinking water analysis.

7. Falsification of data or use of other deceptive practices.

8. Failure to notify the VDH-DWSE VDH-ODW in accordance with 1VAC30-40-30.

1VAC30-40-240. Analytical methodology.

Analytical methods are specified in NPDWR 40 CFR 141 and 143. All procedural steps in the approved methods are considered requirements.

1. Inorganic contaminants. Table III-1 of this chapter shows the approved methodology for inorganic contaminants.

2. Organic contaminants. Table III-2 of this chapter shows the approved methodology for organic contaminants.

3. Secondary inoraganic contaminants. Table III-3 of this chapter shows the approved methodology for secondary inorganic contaminants.

A. Laboratories shall meet the sampling and analytical methodology requirements incorporated by reference at 1VAC30-40-85 B 1 for primary inorganic contaminants, 1VAC30-40-85 B 2 for primary organic contaminants, and 1VAC30-40-85 B 5 for alternative testing methods.

4. Prepackaged kits. B. DPD Colorimetric Test Kit and FACTS Colorimetric Test Kit are the only acceptable prepackaged kits for free chlorine residual.

5. C. Measurement for residual disinfectant, turbidity, pH and temperature need not be made in certified laboratories but may be performed by any persons acceptable by the VDH-DWSE VDH-ODW. The following are the critical elements of these tests:

a. 1. Sealed liquid turbidity standards purchased from the instrument manufacturer shall be calibrated against properly prepared and diluted formazin or styrene divinylbenzene polymer standards at least every four months in order to monitor for any eventual deterioration. This calibration shall be documented. The standards shall be replaced when they do not fall within 15% of the assigned value of the standard. Solid turbidity standards composed of plastic, glass, or other materials shall not be used.

b. 2. Calibration interval for color wheels, sealed ampules, and other visual standards for free chlorine residual at least every six months. These calibrations shall be documented. By comparing standards and plotting such a comparison on graph paper, a correction factor can be derived and applied to all future results obtained on the now calibrated apparatus.

c. 3. Additional criteria. The following criteria shall be used by persons for performing free chlorine residual, turbidity, pH and temperature measurements.

(1) a. Free chlorine residual. Samples shall be collected in plastic or glass. Samples are not preserved; analyses are made within 15 minutes. A DPD or FACTS Colorimetric Test Kit, spectrophotometer or photometer is required.

(2) b. Turbidity. Samples shall be collected in plastic or glass. Samples are not preserved; analyses are to be made within 15 minutes. Nephelometer is needed with light source for illuminating the sample and one or more photoelectric detectors with a readout device to indicate the intensity of light scattered at right angles to the path of the incident light. Unit may be line/bench or battery/portable operated.

(3) c. pH. Samples shall be collected in plastic or glass. Samples are not preserved. Analyses are to be made within 15 minutes. A pH meter is necessary.

(4) d. Temperature. Samples shall be analyzed immediately. Good A good grade mercury-filled or dial-type centigrade thermometer, or thermistor are is required.

1VAC30-40-250. Sample collection, handling, and preservation.

A. A written sampling procedure with specified sampling instructions shall be made available to sample collectors. The laboratory shall require strict adherence to correct sampling procedures, complete identification of a sample and prompt transfer of the sample to the laboratory.

B. The collector shall be trained in sampling procedures.

C. The sample needs to be representative of the potable water system. The water tap shall be sampled after maintaining a steady water flow for two or three minutes to clear service line unless otherwise specified by the method, as an example, lead and copper. The tap shall be free of any attachments or water purification devices.

D. The sample report form shall be completed immediately after collection with location, date and time of collection, collector's name, preservative added and any remarks concerning the sample. Indelible ink shall be used.

C. E. The sample container, required preservative preservation, and maximum holding time requirements for sampling and analyzing inorganic contaminants are listed in Table III-4 of this chapter incorporated by reference at 1VAC30-40-85 B 1.

D. F. The sample container, required preservative preservation, and maximum holding time requirements for sampling and analyzing organic contaminants are listed in Table III-5 of this chapter incorporated by reference at 1VAC30-40-85 B 2.

G. The sample container, required preservation, and maximum holding time requirements for alternative test methods are incorporated by reference at 1VAC30-40-85 B 5.

E. H. The laboratory shall reject any sample not meeting the above criteria and notify the system or individual requesting the analyses.

1VAC30-40-280. Action response to laboratory results.

When the action response is a designated laboratory responsibility, the laboratory shall notify the proper authority of noncompliance sample results and request resampling from the same sampling point immediately.


TABLE III-1
Approved Methodology for Inorganic Contaminants

Contaminant

Methodology

EPA

ASTM3

SM4

USGS5

Other

Alkalinity

Titrimetric

1 310.1

D1067-88B

2320

1-030-85

_____

Antimony6

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Hydride-Atomic Absorption10

_____

D-3697-87

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Furnace

_____

_____

3113B

_____

_____

Arsenic6

Inductively Coupled Plasma

2 200.7

_____

3120B

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Furnace

2,11 206.2

D-2972-88C

3113B

_____

_____

Hydride Atomic Absorption10

_____

D-2972-88B

3114B

_____

_____

Asbestos

Transmission Electron Microscopy

13 100.1

_____

_____

_____

_____

Transmission Electron Microscopy

14 100.2

_____

_____

_____

_____

Barium6

Inductively Coupled Plasma

2 200.7

_____

3120B

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Direct

_____

_____

3111D

_____

_____

Atomic Absorption; Furnace

1 208.2

_____

3113B

_____

_____

Berryllium6

Inductively Coupled Plasma

2 200.7

_____

3120B

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Furnace

_____

D-3645-84B

3113B

_____

_____

Cadmium6

Inductively Coupled Plasma

2 200.7

_____

_____

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Furnace

_____

_____

3113B

_____

_____

Calcium6

EDTA Titrimetric

1 215.2

D511-88A

3500-Ca-D

_____

_____

Atomic Absorption; Direct Aspiration

1 215.1

D511-88B

3111-B

_____

_____

Inductively Coupled Plasma

2 200.7

_____

3120

_____

_____

Chromium6

Inductively Coupled Plasma

2 200.7

_____

3120B

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Furnace

_____

_____

3113B

_____

_____

Conductivity

Conductance

1 120.1

D1125-82B

2510

_____

_____

Copper6

Atomic Absorption; Furnace

1 220.2

D1688--90C

3113B

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Direct Aspiration

1 220.1

D1688--90A

3111-B

_____

_____

Inductively Coupled Plasma

2 200.7

_____

3120

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Cyanide

Amenable, Spectrophotometric

_____

D2036-91B

4500CN-G

_____

_____

Manual Distillation followed by Spectro.

_____

_____

4500-CN-C16, 18

_____

_____

 

Manual

_____

D2036-91A

4500-CN-E

1-3300-85

_____

 

Semi-automated

9 335.4

_____

_____

_____

_____

 

Selective Electrode

_____

D2036-91A

4500CN-F

_____

_____

Fluoride

Ion Chromatography

9 300.0

D4327-91

4110B

_____

_____

Manual Distill; Color. SPADNS

_____

_____

4500F-B,D

_____

_____

Manual Electrode

_____

D1179-88B

4500F-C

_____

_____

Automated Electrode

_____

_____

_____

3800-75W E20

_____

Automated Alizarin

_____

_____

4500F-E

_____

129-71W19

Lead6

Atomic Absorption; Furnace Technique

1 239.2

D3559-85D

3113B

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

 

2 200.8

_____

_____

_____

_____

Mercury

Manual, Cold Vapor10

1 245.1

D3223-91

3112B

_____

_____

Automated, Cold Vapor10

1 245.2

_____

_____

_____

_____

Nickel6

Inductively Coupled Plasma

2 200.7

_____

3120B

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Direct

_____

_____

3111B

_____

_____

Atomic Absorption; Furnace

_____

_____

3113B

_____

_____

Nitrate

Ion Chromatography

9 300.0

D4327-91

4110B

_____

B-10118

Automated Cadmium Reduction

9 353.2

D3867-90A

4500-NO3 -F

_____

_____

Ion Selective Electrode

_____

_____

4500-NO3 -D

_____

WeWWG-/58807

Manual Cadmium Reduction

_____

D3867-90B

4500-NO3 -E

_____

_____

Nitrite

Ion Chromatography

9 300.0

D4327-91

4110B

_____

B-10118

Automated Cadmium Reduction

9 353.2

D3887--90A

4500-NO3--F

_____

_____

Manual Cadmium Reduction

_____

D3867-90B

4500-NO3--E

_____

_____

Spectrophotometric

1 354.1

_____

_____

_____

_____

O-Phosphate Unfiltered, no digestion or hydrolysis

Colorimetric: Ascorbic Acid

_____

_____

_____

_____

_____

 

Manual; 2 Reagent

1 365.3

_____

_____

_____

_____

 

Manual; 1 Reagent

1 365.2

D515-88A

4500-P-E

_____

_____

 

Auto; Segmented

_____

_____

_____

1-2601-85

_____

 

Auto; Discrete

_____

_____

_____

1-2598-85

_____

Ion Chromatography

9 300.0

D4327-91

4110B

_____

_____

pH

Electrometric - Individual Measurement

1 150.1

D1293-84B

4500-H

_____

_____

Electrometric - Online Measurement

1 150.2

_____

_____

_____

_____

Residual Disinfectant Chlorine

Amperometric Titration

_____

_____

4500C1-D

_____

_____

Amperometric Titration- low level

_____

_____

4500C1-E

_____

_____

DPD Colorimetric Method

_____

_____

4500C1-G

_____

_____

DPD Titrimetric

_____

_____

4500C1-F

_____

_____

Syringaldazine (FACTS)

_____

_____

4500C1-H

_____

_____

Ozone Chlorine Dioxide

Indigo Method

_____

_____

4500O3 B

_____

21

Amperometric Method

_____

_____

4500C102

_____

_____

DPD Colorimetric

_____

_____

4500C102 -D

_____

_____

Amperometric Method

_____

_____

4500C102 -E

_____

_____

Selenium6

Hydride-Atomic Absorption10

_____

D3859-88A

3114B

_____

_____

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Furnace11

_____

D3859-88B

3113B

_____

_____

Silica
filtered

Colorimetric-Molybdate Blue-Manual

1 370.1

D89-88

_____

1-700-85

_____

Automated

_____

_____

_____

1-2700-85

_____

Molybdosilicate-Manual

_____

_____

4500Si-D

_____

_____

Heteropoly Blue-Manual

_____

_____

4500Si-E

_____

_____

Molybdate Reactive Silica-Automated

_____

_____

4500Si-F

_____

_____

Inductively Coupled Plasma

2 200.7

_____

3120

_____

_____

Sodium6

Atomic Absorption: Direct Aspiration

1 273.1

_____

_____

_____

_____

Inductively Coupled Plasma

2 200.7

_____

3120

_____

_____

Flame Photometric

_____

D1428-82A

3500Na-D

_____

_____

Temperature

Thermometric

_____

_____

2550

_____

_____

Thallium6

ICP-Mass Spectrometry

2 200.8

_____

_____

_____

_____

Atomic Absorption; Platform

2 200.9

_____

_____

_____

_____

Atomic Absorption; Furnace

_____

_____

3113B

_____

_____

Turbidity

Nephelometric

1 180.1

_____

2130B

_____

_____

Great Lake Instruments

_____

_____

_____

_____

Method 2

1 Methods for Chemical Analysis of Water and Wastes, EPA-600/4-79-020, March 1983. Available at NTIS, publication order number PB84-128677.

2 Methods for the Determination of Metals in Environmental Samples. EPA-600/4-91-010. Available at NTIS, PB 91-231498, June 1991.

3 Annual Book of ASTM Standards, Vols. 11.01 and 11.02, 1993, American Society for Testing and Materials, 1918 Race Street, Philadelphia, PA 19103.

4 18th edition of Standard methods for the Examination of Water and Wastewater, 1992, American Public Health Association, American Water Works Association, Water Environment Federation.

5 Techniques of Water Resources Investigations of the U.S. Geological Survey, Book 5, Chapter A-1, Third Edition, 1989. Available at Superintendent of Documents, U.S. Government printing Office, Washington, DC 20402.

6 Samples may not be filtered. Samples that contain less than 1 NTU(ne phelometric turbidity unit) and are properly preserved (concentrated nitric acid to pH <2) may be analyzed directly (without digestion) for total metals; otherwise, digestion is required. Turbidity must be measured on the preserved samples just prior to the initiation of metal analysis. When digestion is required, the total recoverable technique as defined in the method must be used.

7 Orion Guide to Water and Wastewater Analysis, Form WeWWG/5880, p. 5, 1985. Orion Research, Inc., Cambridge, MA.

8 Waters Test Method for Determination of Nitrite/Nitrate in Water Using Single Column Ion Chromatography, Method B-1011, Millipore Corporation, Waters Chromatography Division, 34 Maple Street, Milford, MA 01757.

9 Methods for the Determination of Inorganic Substances in Environmental Samples, EPA/600/R/93/100, August 1993. Environmental Monitoring Systems Laboratory, Cincinnati, OH 45268.

10 For the Gaseous hydride determinations of antimony, arsenic, and selenium and for the determination of mercury by the cold vapor techniques, the proper digestion technique as defined in the method must be followed to ensure the element is in the proper state for analysis.

11 Add 2 ml of 30% hydrogen peroxide and an appropriate concentration of matrix modifier nickel nitrate to samples.

13 Method 100.1 Analytical method for Determination of Asbestos, Fibers in Water, EPA-600/4-83-043, September 1983, U.S. EPA Environmental Research Laboratory, Athena, GA 30613. Available at NTIS, PB 83-260471.

14 Method 100.2 Method for the Determination of Asbestos Structure over 10 pm in Length in Drinking Water, (1993), Technical Support division, Cincinnati, OH 45268.

16 The distillation procedure in EPA Method 335.2 should not be used.

18 EPA Methods 335.2 and 335.3 require the sodium hydroxide absorber solution final concentration to be adjusted to 0.25 N before colorimetric analysis.

19 Fluoride in Water and Wastewater. Industrial Method No. 129-71-W. Technicon Industrial Systems. Tarrytown, NY 10591 December 1972.

20 Fluoride in Water and Wastewater, Method No. 380-75WE. Technicon Industrial Systems. Tarrytown, NY 10591, February 1976.

 

Table III-2
Approved Methodology for Organic Contaminants

Contaminant

EPA Method

Total Trihalomethanes (TTHM)

502.2, 524.2, 551

Maximum Trihalomethane Potential (MTP)

510.1

Benzene

502.2, 524.2

Carbon tetrachloride

502.2, 524.2, 551.

1,2-Dichlorobenzene

502.2, 524.2

1,4-Dichlorobenzene

502.2, 524.2

1,2-Dichloroethane

502.2, 524.2

cis-Dichloroethylene

502.2, 524.2

trans-Dichloroethylene

502.2, 524.2

Dichloromethane

502.2, 524.2

1,2-Dichloropropane

502.2, 524.2

Ethylbenzene

502.2, 524.2

Styrene

502.2, 524.2

Tetrachloroethylene

502.2, 524.2, 551.

1,1,1-Trichloroethane

502.2, 524.2, 551.

Trichloroethylene

502.2, 524.2, 551.

Toluene

502.2, 524.2.

1,2,4-Trichlorobenzene

502.2, 524.2.

1,1-Dichloroethylene

502.2, 524.2.

1,1,2-Trichloroethane

502.2, 524.2

Vinyl chloride

502.2, 524.2.

Xylene (total)

502.2, 524.2.

2,3,7,8-TCDD (dioxin)

1613.

2,4-D

515.2, 555.

2,4,5-TP (Silvex)

515.2, 555.

Alachlor

505, 507 2, 525.2.

Atrazine

505, 507 2, 525.2.

Benzo(a)pyrene

525.2, 550, 550.1.

Carbofuran

531.1

Chlordane

531.1

Dalapony

552.1

Di(2-ethylhexyl)adipate

506, 525.2.

Di(2-ethylhexyl)phthalate

506, 525.2.

Dibromochloropropane (DBCP)

504, 551.

Dinoseb

515.2, 555.

Diquat

549.1

Endothal

548.1

Endrin

505, 508 2, 525.2.

Ethylenedibromide (EDB)

504, 551.

Glyphosate

547, 6651 1.

Heptachlor

505, 508 2, 525.2.

Heptachlor Epoxide

505, 508 2, 525.2.

Hexachlorobenzene

505, 508 2, 525.2.

Hexachlorocyclopentadiene

505, 525.2

Lindane

505, 508 2, 525.2

Methoxychlor

505,508 2, 525.2

Oxamyl

531.1.

PCBs 3 (as decachlorobiphenyl)

508A

 

(as Aroclors)

505, 508 2

Pentachlorophenol

515.2, 525.2, 555

Picloram

515.2, 555.

Simazine

505, 507 2, 525.2

Toxaphene

508 2, 525.2

Aldicarb

531.1

Aldicarb sulfone

531.1.

Aldicarb sulfoxide

531.1.

Aldrin

505, 508 2, 525.2.

Butachlor

507 2, 525.2.

Carbaryl

531.1.

Dicamba

515.2, 555.

Dieldrin

505, 508 2, 525.2.

3-hydroxycarbofuran

531.1.

Methomyl

531.1.

Metholachlor

507 2, 525.2.

Metribuzin

507 2, 525.2.

Propachlor

508 2, 525.2.

1 Method 6651 is contained in the 18th edition of Standard Methods for the Examination of Water and Wastewate, 1992, American Public Health Association, Water Works Association, Water Environmental Federation.

2 Solid phase extraction procedures, as specified in USEPA Method 525.2, may be used as an option with USEPA Methods 507 and 508.

3 PCBs are qualitatively identified as Aroclors and measured for compliance purposes as decachlorobiphenyl.

 

Table III-3
Approved Methodology for Secondary Inorganic Contaminants

Containment

EPA

ASTM 3

SM 4

Other

Aluminum 6

2 200.7

 

3120B

 

 

2 200.8

 

 

 

 

2 200.9

 

3113B

 

 

 

 

3111D

5 1-305-85

Chloride

8 300.0

4327-91

4110

 

 

 

 

4500-C1-D

 

Color

1 110.2

 

2120B

 

Copper 6

2 200.7

 

3120B

 

 

2 200.8

 

 

 

 

2 200.9

 

 

 

 

1 200.1

D1688-90A

3111B

 

 

1 200.2

D1688-90C

3113B

 

Flouride

8 300.0

D4327-91

4110

 

 

 

D1179-88A

4500F-B

 

 

 

D1179-88B

and D